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    The dried samples were completely smashed using ultrafine grinder (Cerendiptor MKCA 63, Masuko, Japan) and filtered with 200 mesh number sieve. The accurately weighed samples were treated with 40% NaOH ( w / w ) at 100 °C for 1 h to remove proteins, and then soaked in 5% HCl ( w / w ) solution with rotation at 750 rpm for 24 h at ambient temperature to remove CaCO 3 and other minerals.

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     · at 6,000 rpm for 15 min. CNFs were then isolated by mechanical fibrillation using an ultrafine grinder (MKCA 6–3 from Masuko, Japan) at 1,440 rpm for 30 min, followed by a high pressure homogeniser (Model 2000, APV, Denmark) as described in). ...

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    pulp with a 2.0 wt% concentration was passed through an ultrafine grinder (Supermasscolloider MKCA 6-2J CE, Masuko Sangyo Co., Ltd., Kawaguchi, Japan) until a final gap of −90 µm relative to the initial contact point of the grinding stones was

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    Ultrafine Friction Grinder Tests e to g were processed with an ultra-fine friction grinder (Supermasscolloider from Masuko Sangyo Co. Ltd, Japan (Model MKCA 6-2) with mounted silicon carbide stones having a grit class of 46 (grit size 297-420 μm).

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     · 1. ULTRAFINE GRINDERS. 2. CONTENT • Ultrafine grinders • Classifying hammer mills • Fluid energy mills • Agitated mills. 3. ULTRAFINE GRINDERS • Many commercial powders must contain particles averaging 1 to 20 µm in size, with substantially all particles passing a standard 325-mesh screen that has openings 44 µm wide.

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     · Subsequently, unmodified nanofibrils, herein termed CNF-0, were obtained by grinding the suspension with an ultrafine grinder (MKCA 6-3, Masuko Sangyo, Kawaguchi, Japan). Preparation of phosphorylated CNF

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     · pulp with a 2.0 wt% concentration was passed through an ultrafine grinder (Supermasscolloider MKCA 6-2J CE, Masuko Sangyo Co., Ltd., Kawaguchi, Japan) until Figure 1. Process schematic. Ice-templating was used to orient the cellulose nanofibers (CNFs

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     · Then, 1.0 wt% pulp suspension was nano-disintegrated using a commercial ultrafine grinder (MKCA 6-2, Masuko Sangyo Co., Ltd., Japan) to obtain nanofibrils. The slurry passed through two grinding discs 10 times with a disc gap of -100 microns at 2000 rpm.

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    Ultrafine grinding or nanosizing terms were frequently used for the process, when the size of the particle lies in the range of nanometers compared to the other synthesis method. Mechanical attrition methods lead to higher production rates (tons of nanomaterials can be produced in an hour) and widely used in industrial production like metal, clay, and coal powders [22–28] .

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